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The University of Oxford’s Materials Department uses Deben μXCT stages to characterise engineering materials.

Professor James Marrow leads a research group specialising in the structure-property relationship of a broad range of engineering and natural materials.  Based  in  the  Materials  Department  at  the University of Oxford, Marrow’s team use high resolution X-ray computed tomography to make in situ studies  of  three-dimensional  deformation  and  damage (e.g. digital volume  correlation),  with  a particular interest in materials for energy.  Research in engineering materials for energy generation is not a quick-fix topic.  New  materials  can  take  from  15-20  years  to  come  into  use  and  then  are expected to be in service for 40-80 years. The key physical mechanisms that determine manufactured performance, and how these properties age in service, are not very well understood, and mistakes in materials selection can have enormous financial and social implications.  Prediction is a major challenge and thus a deep understanding of the fundamental mechanisms of materials aging and how it affects damage tolerance is essential to identify and avoid potential “cliff-edges” in future materials performance. Testing is based in house and using the Diamond Light Source synchrotron x-ray facility at Harwell. The range of materials studied is quite remarkable; from graphite and ceramic composites for nuclear energy to interfacially-toughened polymer composite laminates for aerospace; from the study of eggs shells to samples of human bone. With experiments running from a few hours to several days, it does not come as a surprise to learn that the CT facility is running 24/7. The micro CT system is a ZEISS Xradia 510 Versa.  This  provides  a  two-stage  magnification  technique  to  enable  high  resolution  at  a distance (RaaD). In the first stage, the sample image is enlarged through geometric magnification as with conventional micro-CT. In the second stage, a scintillator converts X-rays to visible light, which is then optically magnified.  Reducing dependence upon geometric magnification enables the Versa to maintain submicron resolution at large working distances, which is essential for in situ observations of mechanical testing. The  figure  shows  a  silicon-carbide  ceramic  composite  that is  designed for future  accident  tolerant nuclear  fuels.

In situ mechanical loading has been applied to create an internal pressure, which eventually initiates cracks from the larger pores within its woven structure.   The digital volume correlation analysis of the tomographs reveals cracks as strains (colour), and the sequence and pattern of their nucleation and growth is used to test high fidelity models that predict how changes in microstructure affect the structural integrity of the material.1,2

The  Deben  Microtest  CT  tensile  stages  for  μXCT  systems  allow  samples  to  be  examined  using customised load cells in the range from 150 N up to 5000 N (5kN). Custom versions are available with Peltier heating & cooling from -20 °C to +160 °C, extended stroke and travel.

The  Deben  CT5000  stage  (left)  mounted  on an  experimental  system  at the  Diamond  Light Source  at  Harwell.  (photograph  courtesy  of James Marrow)

References

1 Saucedo-Mora, L., Lowe, T., Zhao, S., Lee, P. D., Mummery, P. M., & Marrow, T. J. (2016). In situ observation of mechanical damage within a SiC-SiC ceramic matrix composite. Journal of Nuclear Materials, 481, 13–23. https://doi.org/10.1016/j.jnucmat.2016.09.007

2 Saucedo-Mora, L., & Marrow, T. J. (2016). Multi-scale damage modelling in a ceramic matrix composite using a finite-element microstructure meshfree methodology. Philosophical Transactions of the Royal Society of London A: Mathematical, Physical and Engineering Sciences, 374(2071). https://doi.org/10.1098/rsta.2015.0276

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